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Please use this identifier to cite or link to this item: https://hdl.handle.net/1959.11/22907
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dc.contributor.authorWilkinson, Brendanen
dc.contributor.authorFairbanks, Antony Jen
dc.date.accessioned2018-04-27T09:52:00Z-
dc.date.issued2008-
dc.identifier.citationTetrahedron Letters, 49(33), p. 4941-4943en
dc.identifier.issn1873-3581en
dc.identifier.issn0040-4039en
dc.identifier.urihttps://hdl.handle.net/1959.11/22907-
dc.description.abstractA general and efficient one-pot method for the synthesis of carbohydrate thionolactones from the corresponding 1-thiosugar is described involving the formation of an intermediate glycosyl S-tert-butyl thiosulfinate in situ by treatment of a thiol with commercially available tert-butylsulfinyl chloride in toluene at room temperature, followed by thermolysis. The method can also be used to generate reactive thioaldehydes and thioketones directly from thiols, which can be trapped in situ with a suitable diene.en
dc.languageenen
dc.publisherElsevier Ltden
dc.relation.ispartofTetrahedron Lettersen
dc.titleOne-pot synthesis of carbohydrate thionolactones from 1-thiosugarsen
dc.typeJournal Articleen
dc.identifier.doi10.1016/j.tetlet.2008.05.145en
dc.subject.keywordsOrganic Chemical Synthesisen
local.contributor.firstnameBrendanen
local.contributor.firstnameAntony Jen
local.subject.for2008030503 Organic Chemical Synthesisen
local.subject.seo2008970103 Expanding Knowledge in the Chemical Sciencesen
local.profile.schoolSchool of Science and Technologyen
local.profile.emailbwilkin7@une.edu.auen
local.output.categoryC1en
local.record.placeauen
local.record.institutionUniversity of New Englanden
local.identifier.epublicationsrecordune-20180425-10087en
local.publisher.placeUnited Kingdomen
local.format.startpage4941en
local.format.endpage4943en
local.identifier.scopusid46049118601en
local.peerreviewedYesen
local.identifier.volume49en
local.identifier.issue33en
local.contributor.lastnameWilkinsonen
local.contributor.lastnameFairbanksen
dc.identifier.staffune-id:bwilkin7en
local.profile.orcid0000-0003-1866-6540en
local.profile.roleauthoren
local.profile.roleauthoren
local.identifier.unepublicationidune:23091en
local.identifier.handlehttps://hdl.handle.net/1959.11/22907en
dc.identifier.academiclevelAcademicen
local.title.maintitleOne-pot synthesis of carbohydrate thionolactones from 1-thiosugarsen
local.output.categorydescriptionC1 Refereed Article in a Scholarly Journalen
local.search.authorWilkinson, Brendanen
local.search.authorFairbanks, Antony Jen
local.uneassociationUnknownen
local.year.published2008en
local.subject.for2020340503 Organic chemical synthesisen
local.subject.seo2020280105 Expanding knowledge in the chemical sciencesen
local.codeupdate.date2022-02-13T16:58:56.670en
local.codeupdate.epersonbwilkin7@une.edu.auen
local.codeupdate.finalisedtrueen
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